NMR Spectroscopy Service
Off
Services
The NMR facility in the Department of Chemistry is equipped with five instruments at 400MHz (4) and 500MHz (1), capable of performing a range of measurements, including:
- standard 1H and 13C measurements
- multinuclear NMR (e.g. 2H, 11B, 19F, 29Si, 31P etc.)
- variable temperature (above and below ambient)
- 2D NMR (e.g. HSQC, HMBC, DOSY, etc.)
- routine solid state NMR
We provide expert NMR services to both internal (Chemistry and other UoS Departments) users, as well as external clients (other Universities, commercial customers).
Instruments
- Bruker AVIIIHD 500MHz - "Millicent"
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- 5mm solution state BBFO SmartProbe - 1H / 19F-15N dual resonance, z-gradient
- 4mm solid state 1H(19F) / 31P-15N dual resonance
- Bookable instrument for trained users
- Bruker AVIIIHD 400MHz - "Magnus"
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- 5mm solution state BBFO SmartProbe - 1H / 19F-15N dual resonance, z-gradient
- Open-access instrument for trained users
- Bruker AVIII 400MHz - "Marmaduke"
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- 5mm solution state BBFO - 1H / 19F-15N dual resonance, z-gradient
- Bookable instrument for trained users
- Bruker AV 400 MHz - "Monty"
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- 5 mm solution state BBFO SmartProbe - 1H / 19F-15N dual resonance, z-gradient
- Open-access instrument for trained users
- Spinsolve 60 Benchtop NMR spectrometer
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- 5 mm solution state probe 1H, 19F, 31P
- Flow cell for continuous reaction monitoring
- 20 position sample changer
- Open access instrument for undergraduate use in teaching labs
All instruments are equipped with 60-position sample changer for solution state samples.
Contact
To discuss your requirements please get in touch with our NMR specialist Dr Khalid Doudin.
Email: k.doudin@sheffield.ac.uk
Phone: +44 (0)114 222 9312